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Dicyclopentyl azodicarboxylate (DCpAD):A new alternative azo-reagent for the Mitsunobu reaction |
Jian Hai Yang, Li Yan Dai, Xiao Zhong Wang, Ying Qi Chen |
Department of Chemical and Biological Engineering, Zhejiang University, Hangzhou 310027, China |
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Abstract Dicyclopentyl azodicarboxylate is introduced as a new azo-reagent which can be conveniently prepared in two steps and be used in the Mitsunobu reaction. Though there are no distinct difference of reactivity between DCpAD and DEAD, the former is a more preferable azo-reagent for its stability.
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Received: 07 December 2010
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Corresponding Authors:
Li Yan Dai,E-mail address:dailiyan@zju.edu.cn
E-mail: dailiyan@zju.edu.cn
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About author:: 10.1016/j.cclet.2011.03.017 |
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