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Synthesis of di-μ-oxo-tetra-(α-pentyloxy) tin(IV) phthalocyanine |
Yi Ru Peng, Yu Hong Cao, Pei Feng Chen, Xiao Xia Huang |
College of Chemistry & Material Science, Fujian Normal University, Fuzhou 350007, China |
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Abstract Axially substituted tin phthalocyanines, namely dichloride-tetra-(α-pentyloxy) tin (IV) phthalocyanine 2, dihydroxy-tetra-(α-pentyloxy) tin (IV) phthalocyanine 3 and its dimmer di-μ-oxo-tetra-(α-pentyloxy) tin (IV) phthalocyanine 4 were synthesized. The catalytic effect of H2O-free CaCl2 in quinoline was used for condensation of dihydroxy tin phthalocyanine 3 to the cofacially arraydimmer 4. Their structures were characterized by UV-vis, IR, elemental analysis, MS, as well as 1HNMR spectroscopy.
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Received: 24 September 2007
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Fund:This study was supported by the National Natural Science Foundation of China (No. 20604007), Natural Science Foundation of Fujian (No. C0510007), Key Foundation for Ministry of Education, China (No. 206071), Key Foundation for Technology Department (2007I0013), Key Foundation for Education Office of Fujian (No. JA05195). |
Corresponding Authors:
Yi Ru Peng,E-mail address:yirupeng@hotmail.com
E-mail: yirupeng@hotmail.com
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